System: Automated laboratory scale rectification system
Evaporator: Round flask with electric Heater, 750 Watt
Column: DN30/40/50, with trays or as packed column
Materials: Glass, PTFE, PVDF, stainless steel
Reflux divider: Funnel with solenoid drive Phase separator Manually adjustable
Vacuum: Dry membrane pump, 2.3 m³/h, 10 mbar
Feed: Membrane dosing pump
Product vessels: 3 x 3 l round flask
Cooling: water cooled
Control system
The control system is an industrial Siemens Process Logical Controller (PLC). The operation system is a standard PC with the visualization (HMI) software Simatic WinCC.
The system can be delivered with PI(D)- controllers for energy, feed, vacuum, reflux-ratio, differential pressure, temperature evaporator, head temperature, feed temperature.
The set point can be adjusted by the operator. The controller structure and parameters can be adjusted at administrator level.
Technical Data:
Manufacturer: AP-Miniplant GmbH & Co. KG
EU-directives: 73/23/EC Low-voltage directive 89/336/EC Electromagnetic compliance
Operating pressure range: -1 – 0.2 bar overpressure
Operating temperature range: -10 – 200 °C
Ambient temperature range: 5 – 40 °C
Storage temperature range: 0 – 55 °C
Max. humidity at 40 °C / 20 °C 50 % / 90%
Plant weight 550 kg
Plant size (LxWxH) 1560 x 660 x 2360 mm
Electrical supply AC 230V / 50/60Hz +- 10 %, 1 phase system without
neutral conductor
Main fuse 16 A (automatic circuit-breaker)
Residual Current device 1x 25 A, 30 mA for heating
1x 25A, 300mA for all other components
Electrical power Max. ~ 3 kW
Water supply pressure 1 – 3 bar
Fresh water flow rate 15 l/min
Nitrogen supply pressure max.: 10 bar
Compressed air: 6-8 bar
Noise level: < 70 dB(A)
Technical Data:
Manufacturer: AP-Miniplant GmbH & Co. KG
EU-directives: 73/23/EC Low-voltage directive 89/336/EC Electromagnetic compliance
Operating pressure range: -1 – 0.2 bar overpressure
Operating temperature range: -10 – 200 °C
Ambient temperature range: 5 – 40 °C
Storage temperature range: 0 – 55 °C
Max. humidity at 40 °C / 20 °C 50 % / 90%
Plant weight 550 kg
Plant size (LxWxH) 1560 x 660 x 2360 mm
Electrical supply AC 230V / 50/60Hz +- 10 %, 1 phase system without
neutral conductor
Main fuse 16 A (automatic circuit-breaker)
Residual Current device 1x 25 A, 30 mA for heating
1x 25A, 300mA for all other components
Electrical power Max. ~ 3 kW
Water supply pressure 1 – 3 bar
Fresh water flow rate 15 l/min
Nitrogen supply pressure max.: 10 bar
Compressed air: 6-8 bar
Noise level: < 70 dB(A)
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